Sinthesis and Properties of Hard Carbon Materials Made of Molybdenum-Doped Viscose Fiber for Negative Electrodes of Sodium-Ion Batteries

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Рұқсат ақылы немесе тек жазылушылар үшін

Аннотация

Herein, a method for the preparation of hard carbon via carbonization of chemically modified (molybdenum-doped) commercially available viscose fiber was developed. The effects of a molybdenum dopant on carbonization conditions were studied. The carbonization products retained the fibrous structure and flexibility. The structural features of the synthesized hard carbon materials were investigated, and their relationships to the carbonization temperature and the amount of the molybdenum dopant were analyzed. The texture of materials was studied, and correlations between the specific surface area and porosity, on the one hand, and the synthesis conditions, on the other, were discovered. The usefulness of the products as anode materials for sodium-ion batteries was evaluated. The electrochemical tests, together the extant relevant data, indicate that molybdenum induces the structural rearrangement of the carbon framework upon annealing, accompanied by the growth and ordering of graphite-like nanoclusters. The material prepared at 1050°C exhibited the best electrochemical performances among the synthesized products and the stable cyclability with a capacity of 290 (mA h)/g at a current density of 25 mA/g.

Авторлар туралы

V. Zheleznov

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

N. Saenko

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

V. Maiorov

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

A. Ustinov

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

T. Sokol’nitskaya

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

V. Kuryavyi

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

D. Shlik

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

A. Sokolov

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

D. Opra

Institute of Chemistry, Far Eastern Branch, Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: ttt@ich.dvo.ru
690022, Vladivostok, Russia

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Қосымша файлдар


© В.В. Железнов, Н.С. Саенко, В.Ю. Майоров, А.Ю. Устинов, Т.А. Сокольницкая, В.Г. Курявый, Д.Х. Шлык, А.А. Соколов, Д.П. Опра, 2023