"2+1" Technetium and Rhenium Tricarbonyl Complexes with N,N′-Bidentate Ligands and Methyl 11-Isocyanoundecanoate

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Abstract

«2+1» tricarbonyl complexes [M(CO)3(N^N)CN(CH2)10COOMe]ClO4, where M = Tc or Re and N^N = 2,2′-bipridine (bipy) or 1,10-phernanthroline (phen), were prepared by reaction of [M(CO)3(N^N)(MeOH)]ClO4 with methyl 11-isocyanoundecanoate in methanol. The complexes were isolated and characterized by IR, 1H NMR spectroscopy and elemental analysis. Stability of the «2+1» tricarbolyl complexes with respect to transchelation with histidine was studied.

About the authors

A. E Miroslavov

Khlopin Radium Institute;St. Petersburg State University;Ozersk Technological Institute of the National Research Nuclear University

A. P Sakhonenkova

Khlopin Radium Institute;St. Petersburg State University;Ozersk Technological Institute of the National Research Nuclear University

M. Yu. Tyupina

Khlopin Radium Institute;Ozersk Technological Institute of the National Research Nuclear University;St. Petersburg State Pediatric Medical University

Email: mtupina@mail.ru

G. V Sidorenko

Khlopin Radium Institute

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